Confidence Report: Unterschied zwischen den Versionen
Cbier (Diskussion | Beiträge) Keine Bearbeitungszusammenfassung |
Cbier (Diskussion | Beiträge) Keine Bearbeitungszusammenfassung |
||
Zeile 2: | Zeile 2: | ||
To perform a System Suitability Test or a Data Diagnosis, you must set up the corresponding section in the Confidence Report and also the Component Table. If either one is not set up, the calculation is not performed. | To perform a System Suitability Test or a Data Diagnosis, you must set up the corresponding section in the Confidence Report and also the Component Table. If either one is not set up, the calculation is not performed. | ||
Tool Bar Shortcut | '''Tool Bar Shortcut''' | ||
Click on [[File:Confidence Format.png]]. | Click on [[File:Confidence Format.png]]. | ||
Zeile 9: | Zeile 9: | ||
!'''Dialog Box Options''' !! | !'''Dialog Box Options''' !! | ||
|- | |- | ||
|style="width: | |style="width:130px;text-align:left; vertical-align:top;"|'''Content''' | ||
|style="width:525px;text-align:left; vertical-align:top;"|Select one or more of the following: | |style="width:525px;text-align:left; vertical-align:top;"|Select one or more of the following: | ||
:'''System Suitability Test:''' Check to enable the System Suitability Test section for setup. | :'''System Suitability Test:''' Check to enable the System Suitability Test section for setup. | ||
Zeile 15: | Zeile 15: | ||
:'''Data Diagnosis:''' Check to enable Data Diagnosis section for setup. | :'''Data Diagnosis:''' Check to enable Data Diagnosis section for setup. | ||
|- | |- | ||
|style="width:150px;text-align:left; vertical-align:top;"|'''System Suitability Test''' Check to perform SST. | |style="width:150px;text-align:left; vertical-align:top;"|'''System Suitability Test''' | ||
Check to perform SST. | |||
|style="width:525px;text-align:left; vertical-align:top;"|'''Calculate using:''' Select '''Full Width (USP)''' to have SST parameters calculated using peak width at the baseline. Select '''Half Width (EUP)''' or '''Half Width (JP)''' to have SST parameters calculated using peak width at half peak height. | |style="width:525px;text-align:left; vertical-align:top;"|'''Calculate using:''' Select '''Full Width (USP)''' to have SST parameters calculated using peak width at the baseline. Select '''Half Width (EUP)''' or '''Half Width (JP)''' to have SST parameters calculated using peak width at half peak height. | ||
Zeile 22: | Zeile 24: | ||
'''Criteria for Warning: Asymmetry (As), No. of Theoretical Plates (N), Resolution (R)''', and Signal to Noise Ratio '''(S/N)''' can be used as criteria for System Suitability checking. See: System Suitability Tests (SST) for more information on these parameters. | '''Criteria for Warning: Asymmetry (As), No. of Theoretical Plates (N), Resolution (R)''', and Signal to Noise Ratio '''(S/N)''' can be used as criteria for System Suitability checking. See: System Suitability Tests (SST) for more information on these parameters. | ||
|- | |- | ||
|style="width:150px;text-align:left; vertical-align:top;"|'''Module Performance Test''' Check to perform the Module Performance Test. | |style="width:150px;text-align:left; vertical-align:top;"|'''Module Performance Test''' | ||
Check to perform the Module Performance Test. | |||
|style="width:525px;text-align:left; vertical-align:top;"|The '''Module Performance Test''' is not available when the D-6000 I/F is selected on the Method Configuration screen unless the D-6000 is connected to a DAD detector. | |style="width:525px;text-align:left; vertical-align:top;"|The '''Module Performance Test''' is not available when the D-6000 I/F is selected on the Method Configuration screen unless the D-6000 is connected to a DAD detector. | ||
Zeile 33: | Zeile 37: | ||
*The Wavelength difference value from the detector is greater than the specified value. | *The Wavelength difference value from the detector is greater than the specified value. | ||
|- | |- | ||
|style="width:150px;text-align:left; vertical-align:top;"|'''Data Diagnosis''' Check to perform Data Diagnosis. | |style="width:150px;text-align:left; vertical-align:top;"|'''Data Diagnosis''' | ||
Check to perform Data Diagnosis. | |||
|style="width:525px;text-align:left; vertical-align:top;"| '''Diagnosis Peak:''' Check to perform data diagnosis using the diagnosis peak.Enter '''RT(min)''' to specify the retention time of the diagnosis peak, '''Window(%)''' to specify the window for the peak identification, '''Area/Height''' for the expected peak area or height, and '''Tolerance(%)''' for the variation allowed to perform peak diagnosis on the peaks in the STD samples. | |style="width:525px;text-align:left; vertical-align:top;"| '''Diagnosis Peak:''' Check to perform data diagnosis using the diagnosis peak.Enter '''RT(min)''' to specify the retention time of the diagnosis peak, '''Window(%)''' to specify the window for the peak identification, '''Area/Height''' for the expected peak area or height, and '''Tolerance(%)''' for the variation allowed to perform peak diagnosis on the peaks in the STD samples. | ||
'''Expected Conc Peaks:''' Check to perform data diagnosis using E-Conc Components specified in the Component Table. | '''Expected Conc Peaks:''' Check to perform data diagnosis using E-Conc Components specified in the Component Table. | ||
|-|} | |-|} |
Version vom 9. August 2018, 07:47 Uhr
Use this command to set report parameters for System Suitability Tests, Module Performance Tests, and Data Diagnosis. The extent of the report is determined by checking the boxes in the Content group. To perform a System Suitability Test or a Data Diagnosis, you must set up the corresponding section in the Confidence Report and also the Component Table. If either one is not set up, the calculation is not performed.
Tool Bar Shortcut
Click on Datei:Confidence Format.png.
Dialog Box Options | |
---|---|
Content | Select one or more of the following:
|
System Suitability Test
Check to perform SST. |
Calculate using: Select Full Width (USP) to have SST parameters calculated using peak width at the baseline. Select Half Width (EUP) or Half Width (JP) to have SST parameters calculated using peak width at half peak height.
RT of Non-Retained Peak Range: Enter the retention time for the non-retained peak. Criteria for Warning: Asymmetry (As), No. of Theoretical Plates (N), Resolution (R), and Signal to Noise Ratio (S/N) can be used as criteria for System Suitability checking. See: System Suitability Tests (SST) for more information on these parameters. |
Module Performance Test
Check to perform the Module Performance Test. |
The Module Performance Test is not available when the D-6000 I/F is selected on the Method Configuration screen unless the D-6000 is connected to a DAD detector.
Print Pressure/Temperature Profile: Check to have pressure and temperature profiles of L-7100 (pump) and L-7300 (oven) used plotted in the report. Note that pressure profiles are not available if the pump table has only one step (see Pump Setup). Criteria for Warning: Set up the threshold parameters for warnings by checking Injections to Column, Pressure at Start Time, Lamp Energy at Start Time, and Wavelength Accuracy. Note that for DAD detectors (except the L-7455), Wavelength Accuracy is disabled. The HSM prints the corresponding warning messages in the report if any of the following occurs:
|
Data Diagnosis
Check to perform Data Diagnosis. |
Diagnosis Peak: Check to perform data diagnosis using the diagnosis peak.Enter RT(min) to specify the retention time of the diagnosis peak, Window(%) to specify the window for the peak identification, Area/Height for the expected peak area or height, and Tolerance(%) for the variation allowed to perform peak diagnosis on the peaks in the STD samples.
Expected Conc Peaks: Check to perform data diagnosis using E-Conc Components specified in the Component Table. |